Structural changes induced by Sn, Zr, Al substitution in ZnkIn2Ok+3 transparent conducting oxides powders as deduced by transmission electron microscopy
Identifieur interne : 010910 ( Main/Repository ); précédent : 010909; suivant : 010911Structural changes induced by Sn, Zr, Al substitution in ZnkIn2Ok+3 transparent conducting oxides powders as deduced by transmission electron microscopy
Auteurs : RBID : Pascal:01-0364220Descripteurs français
- Pascal (Inist)
- Etude expérimentale, Poudre, Préparation chimique, Réaction état solide, Oxyde Mixte, Zinc oxyde, Indium oxyde, Matériau transparent, Matériau conducteur, Substitution ion, Etain oxyde, Aluminium oxyde, Zirconium oxyde, Cristallochimie, Structure cristalline, Microstructure, Diffraction RX, Diagramme poudre, TEM, Solution solide, Composition chimique, Polytypisme, Intercroissance, Haute résolution, Al In O Zn, 6166F, ZnkIn2Ok+3, In O Zn, In O Sn Zn, In O Zn Zr.
English descriptors
- KwdEn :
- Aluminium oxides, Chemical composition, Chemical preparation, Conducting materials, Crystal chemistry, Crystal structure, Experimental study, High-resolution methods, Indium oxides, Intergrowth, Ion substitution, Microstructure, Oxides Mixed, Polytypism, Powder pattern, Powders, Solid solutions, Solid state reaction, TEM, Tin oxides, Transparent material, XRD, Zinc oxides, Zirconium oxides.
Abstract
Sn, Zr and Al substituted ZnkIn2Ok+3 powders were made using high temperature solid state reactions. The resulting samples were first characterized by means of powder X-ray diffraction (XRD) and then by transmission electron microscopy (TEM) to identify the microstructures and phase compositions occasionally occurring within a particle. We found that the substituted powder samples are usually composed of particles made of ZnkIn2Ok+3 polytypes intergrowth mixed with grains of In2O3-type structure, rather than being single phase. From a complete analysis of the collected HRTEM images we obtained a statistical polytype population distribution that was used to satisfactorily simulate the experimental XRD patterns based on Hendricks and Teller approximation.
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en" level="a">Structural changes induced by Sn, Zr, Al substitution in Zn<sub>k</sub>In<sub>2</sub>O<sub>k+3</sub> transparent conducting oxides powders as deduced by transmission electron microscopy</title><author><name sortKey="Maugy, C" uniqKey="Maugy C">C. Maugy</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Laboratoire de Réactivité et Chimie des Solides, Université de Picardie Jules Verne, UPRES-A 6007, 33 rue Saint Leu</s1><s2>80039 Amiens</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Picardie</region><settlement type="city">Amiens</settlement></placeName></affiliation></author><author><name sortKey="Dupont, L" uniqKey="Dupont L">L. Dupont</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Laboratoire de Réactivité et Chimie des Solides, Université de Picardie Jules Verne, UPRES-A 6007, 33 rue Saint Leu</s1><s2>80039 Amiens</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Picardie</region><settlement type="city">Amiens</settlement></placeName></affiliation></author><author><name sortKey="Naghavi, N" uniqKey="Naghavi N">N. Naghavi</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Laboratoire de Réactivité et Chimie des Solides, Université de Picardie Jules Verne, UPRES-A 6007, 33 rue Saint Leu</s1><s2>80039 Amiens</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Picardie</region><settlement type="city">Amiens</settlement></placeName></affiliation></author><author><name sortKey="Guery, C" uniqKey="Guery C">C. Guery</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Laboratoire de Réactivité et Chimie des Solides, Université de Picardie Jules Verne, UPRES-A 6007, 33 rue Saint Leu</s1><s2>80039 Amiens</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Picardie</region><settlement type="city">Amiens</settlement></placeName></affiliation></author><author><name sortKey="Tarascon, J M" uniqKey="Tarascon J">J.-M. Tarascon</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Laboratoire de Réactivité et Chimie des Solides, Université de Picardie Jules Verne, UPRES-A 6007, 33 rue Saint Leu</s1><s2>80039 Amiens</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Picardie</region><settlement type="city">Amiens</settlement></placeName></affiliation></author></titleStmt><publicationStmt><idno type="inist">01-0364220</idno><date when="2001">2001</date><idno type="stanalyst">PASCAL 01-0364220 INIST</idno><idno type="RBID">Pascal:01-0364220</idno><idno type="wicri:Area/Main/Corpus">010A52</idno><idno type="wicri:Area/Main/Repository">010910</idno></publicationStmt><seriesStmt><idno type="ISSN">0022-3697</idno><title level="j" type="abbreviated">J. phys. chem. solids</title><title level="j" type="main">The Journal of physics and chemistry of solids</title></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Aluminium oxides</term><term>Chemical composition</term><term>Chemical preparation</term><term>Conducting materials</term><term>Crystal chemistry</term><term>Crystal structure</term><term>Experimental study</term><term>High-resolution methods</term><term>Indium oxides</term><term>Intergrowth</term><term>Ion substitution</term><term>Microstructure</term><term>Oxides Mixed</term><term>Polytypism</term><term>Powder pattern</term><term>Powders</term><term>Solid solutions</term><term>Solid state reaction</term><term>TEM</term><term>Tin oxides</term><term>Transparent material</term><term>XRD</term><term>Zinc oxides</term><term>Zirconium oxides</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Etude expérimentale</term><term>Poudre</term><term>Préparation chimique</term><term>Réaction état solide</term><term>Oxyde Mixte</term><term>Zinc oxyde</term><term>Indium oxyde</term><term>Matériau transparent</term><term>Matériau conducteur</term><term>Substitution ion</term><term>Etain oxyde</term><term>Aluminium oxyde</term><term>Zirconium oxyde</term><term>Cristallochimie</term><term>Structure cristalline</term><term>Microstructure</term><term>Diffraction RX</term><term>Diagramme poudre</term><term>TEM</term><term>Solution solide</term><term>Composition chimique</term><term>Polytypisme</term><term>Intercroissance</term><term>Haute résolution</term><term>Al In O Zn</term><term>6166F</term><term>ZnkIn2Ok+3</term><term>In O Zn</term><term>In O Sn Zn</term><term>In O Zn Zr</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Sn, Zr and Al substituted Zn<sub>k</sub>In<sub>2</sub>O<sub>k+3</sub> powders were made using high temperature solid state reactions. The resulting samples were first characterized by means of powder X-ray diffraction (XRD) and then by transmission electron microscopy (TEM) to identify the microstructures and phase compositions occasionally occurring within a particle. We found that the substituted powder samples are usually composed of particles made of Zn<sub>k</sub>In<sub>2</sub>O<sub>k+3</sub> polytypes intergrowth mixed with grains of In<sub>2</sub>O<sub>3</sub>-type structure, rather than being single phase. From a complete analysis of the collected HRTEM images we obtained a statistical polytype population distribution that was used to satisfactorily simulate the experimental XRD patterns based on Hendricks and Teller approximation.</div></front></TEI><inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>0022-3697</s0></fA01><fA03 i2="1"><s0>J. phys. chem. solids</s0></fA03><fA05><s2>62</s2></fA05><fA06><s2>8</s2></fA06><fA08 i1="01" i2="1" l="ENG"><s1>Structural changes induced by Sn, Zr, Al substitution in Zn<sub>k</sub>In<sub>2</sub>O<sub>k+3</sub> transparent conducting oxides powders as deduced by transmission electron microscopy</s1></fA08><fA11 i1="01" i2="1"><s1>MAUGY (C.)</s1></fA11><fA11 i1="02" i2="1"><s1>DUPONT (L.)</s1></fA11><fA11 i1="03" i2="1"><s1>NAGHAVI (N.)</s1></fA11><fA11 i1="04" i2="1"><s1>GUERY (C.)</s1></fA11><fA11 i1="05" i2="1"><s1>TARASCON (J.-M.)</s1></fA11><fA14 i1="01"><s1>Laboratoire de Réactivité et Chimie des Solides, Université de Picardie Jules Verne, UPRES-A 6007, 33 rue Saint Leu</s1><s2>80039 Amiens</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ></fA14><fA20><s1>1375-1386</s1></fA20><fA21><s1>2001</s1></fA21><fA23 i1="01"><s0>ENG</s0></fA23><fA43 i1="01"><s1>INIST</s1><s2>8204</s2><s5>354000095614660020</s5></fA43><fA44><s0>0000</s0><s1>© 2001 INIST-CNRS. All rights reserved.</s1></fA44><fA45><s0>15 ref.</s0></fA45><fA47 i1="01" i2="1"><s0>01-0364220</s0></fA47><fA60><s1>P</s1></fA60><fA61><s0>A</s0></fA61><fA64 i1="01" i2="1"><s0>The Journal of physics and chemistry of solids</s0></fA64><fA66 i1="01"><s0>GBR</s0></fA66><fC01 i1="01" l="ENG"><s0>Sn, Zr and Al substituted Zn<sub>k</sub>In<sub>2</sub>O<sub>k+3</sub> powders were made using high temperature solid state reactions. The resulting samples were first characterized by means of powder X-ray diffraction (XRD) and then by transmission electron microscopy (TEM) to identify the microstructures and phase compositions occasionally occurring within a particle. We found that the substituted powder samples are usually composed of particles made of Zn<sub>k</sub>In<sub>2</sub>O<sub>k+3</sub> polytypes intergrowth mixed with grains of In<sub>2</sub>O<sub>3</sub>-type structure, rather than being single phase. From a complete analysis of the collected HRTEM images we obtained a statistical polytype population distribution that was used to satisfactorily simulate the experimental XRD patterns based on Hendricks and Teller approximation.</s0></fC01><fC02 i1="01" i2="3"><s0>001B60A66F1</s0></fC02><fC03 i1="01" i2="3" l="FRE"><s0>Etude expérimentale</s0><s5>01</s5></fC03><fC03 i1="01" i2="3" l="ENG"><s0>Experimental study</s0><s5>01</s5></fC03><fC03 i1="02" i2="3" l="FRE"><s0>Poudre</s0><s5>02</s5></fC03><fC03 i1="02" i2="3" l="ENG"><s0>Powders</s0><s5>02</s5></fC03><fC03 i1="03" i2="3" l="FRE"><s0>Préparation chimique</s0><s5>03</s5></fC03><fC03 i1="03" i2="3" l="ENG"><s0>Chemical preparation</s0><s5>03</s5></fC03><fC03 i1="04" i2="X" l="FRE"><s0>Réaction état solide</s0><s5>04</s5></fC03><fC03 i1="04" i2="X" l="ENG"><s0>Solid state reaction</s0><s5>04</s5></fC03><fC03 i1="04" i2="X" l="SPA"><s0>Reacción estado sólido</s0><s5>04</s5></fC03><fC03 i1="05" i2="X" l="FRE"><s0>Oxyde 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substitution</s0><s5>12</s5></fC03><fC03 i1="10" i2="X" l="SPA"><s0>Sustitución ión</s0><s5>12</s5></fC03><fC03 i1="11" i2="3" l="FRE"><s0>Etain oxyde</s0><s2>NK</s2><s5>13</s5></fC03><fC03 i1="11" i2="3" l="ENG"><s0>Tin oxides</s0><s2>NK</s2><s5>13</s5></fC03><fC03 i1="12" i2="3" l="FRE"><s0>Aluminium oxyde</s0><s2>NK</s2><s5>14</s5></fC03><fC03 i1="12" i2="3" l="ENG"><s0>Aluminium oxides</s0><s2>NK</s2><s5>14</s5></fC03><fC03 i1="13" i2="3" l="FRE"><s0>Zirconium oxyde</s0><s2>NK</s2><s5>15</s5></fC03><fC03 i1="13" i2="3" l="ENG"><s0>Zirconium oxides</s0><s2>NK</s2><s5>15</s5></fC03><fC03 i1="14" i2="3" l="FRE"><s0>Cristallochimie</s0><s5>16</s5></fC03><fC03 i1="14" i2="3" l="ENG"><s0>Crystal chemistry</s0><s5>16</s5></fC03><fC03 i1="15" i2="3" l="FRE"><s0>Structure cristalline</s0><s5>17</s5></fC03><fC03 i1="15" i2="3" l="ENG"><s0>Crystal structure</s0><s5>17</s5></fC03><fC03 i1="16" i2="3" l="FRE"><s0>Microstructure</s0><s5>18</s5></fC03><fC03 i1="16" i2="3" l="ENG"><s0>Microstructure</s0><s5>18</s5></fC03><fC03 i1="17" i2="3" l="FRE"><s0>Diffraction RX</s0><s5>19</s5></fC03><fC03 i1="17" i2="3" l="ENG"><s0>XRD</s0><s5>19</s5></fC03><fC03 i1="18" i2="X" l="FRE"><s0>Diagramme poudre</s0><s5>20</s5></fC03><fC03 i1="18" i2="X" l="ENG"><s0>Powder pattern</s0><s5>20</s5></fC03><fC03 i1="18" i2="X" l="SPA"><s0>Diagrama polvo</s0><s5>20</s5></fC03><fC03 i1="19" i2="3" l="FRE"><s0>TEM</s0><s5>21</s5></fC03><fC03 i1="19" i2="3" l="ENG"><s0>TEM</s0><s5>21</s5></fC03><fC03 i1="20" i2="3" l="FRE"><s0>Solution solide</s0><s5>22</s5></fC03><fC03 i1="20" i2="3" l="ENG"><s0>Solid solutions</s0><s5>22</s5></fC03><fC03 i1="21" i2="3" l="FRE"><s0>Composition chimique</s0><s5>23</s5></fC03><fC03 i1="21" i2="3" l="ENG"><s0>Chemical composition</s0><s5>23</s5></fC03><fC03 i1="22" i2="3" l="FRE"><s0>Polytypisme</s0><s5>24</s5></fC03><fC03 i1="22" i2="3" l="ENG"><s0>Polytypism</s0><s5>24</s5></fC03><fC03 i1="23" i2="X" l="FRE"><s0>Intercroissance</s0><s5>25</s5></fC03><fC03 i1="23" i2="X" l="ENG"><s0>Intergrowth</s0><s5>25</s5></fC03><fC03 i1="23" i2="X" l="SPA"><s0>Intercrecimiento</s0><s5>25</s5></fC03><fC03 i1="24" i2="3" l="FRE"><s0>Haute résolution</s0><s5>26</s5></fC03><fC03 i1="24" i2="3" l="ENG"><s0>High-resolution methods</s0><s5>26</s5></fC03><fC03 i1="25" i2="3" l="FRE"><s0>Al In O Zn</s0><s4>INC</s4><s5>52</s5></fC03><fC03 i1="26" i2="3" l="FRE"><s0>6166F</s0><s2>PAC</s2><s4>INC</s4><s5>56</s5></fC03><fC03 i1="27" i2="3" l="FRE"><s0>ZnkIn2Ok+3</s0><s4>INC</s4><s5>92</s5></fC03><fC03 i1="28" i2="3" l="FRE"><s0>In O Zn</s0><s4>INC</s4><s5>93</s5></fC03><fC03 i1="29" i2="3" l="FRE"><s0>In O Sn Zn</s0><s4>INC</s4><s5>94</s5></fC03><fC03 i1="30" i2="3" l="FRE"><s0>In O Zn Zr</s0><s4>INC</s4><s5>95</s5></fC03><fC07 i1="01" i2="3" l="FRE"><s0>Composé minéral</s0><s5>05</s5></fC07><fC07 i1="01" i2="3" l="ENG"><s0>Inorganic compounds</s0><s5>05</s5></fC07><fC07 i1="02" i2="3" l="FRE"><s0>Métal transition composé</s0><s5>07</s5></fC07><fC07 i1="02" i2="3" l="ENG"><s0>Transition element compounds</s0><s5>07</s5></fC07><fN21><s1>253</s1></fN21></pA></standard></inist></record>Pour manipuler ce document sous Unix (Dilib)
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